- Product Details
Keywords
- 2-Hydroxy-4-methoxybenzophenone-5-sulfonic acid
- 2-Hydroxy-4-methoxybenzophenone-5-sulfonic acid 97%
- 2-Hydroxy-4-methoxybenzophenone-5-sulfonic acid 5-Benzoyl-4-hydroxy-2-methoxybenzene sulfonic aid
Quick Details
- ProName: 2-Hydroxy-4-methoxybenzophenone-5-sulf...
- CasNo: 4065-45-6
- Molecular Formula: C14H12O6S
- Appearance: Pale yellow crystal
- Application: As an anti ultraviolet finishing agent...
- DeliveryTime: in stock
- PackAge: 25kg/drum
- Port: Shanghai
- ProductionCapacity: 100 Kilogram/Day
- Purity: 97%
- Storage: -20°C
- LimitNum: 1 Kilogram
- Grade: Other
Superiority
As an anti ultraviolet finishing agent, it has a good anti-aging and softening effect on cotton fabric and polyester fiber. It is widely used in sunscreen cream, cream, honey, emulsion, oil and other cosmetics. It is a broad spectrum ultraviolet absorber. It has the advantages of high absorption efficiency, innocuity, no teratogenic side effect, good light and thermal stability. It can absorb UV-A and UV-B at the same time. It is the first class sun screening agent approved by FDA in the United States, and its frequency in the United States and Europe is higher than Chemicalbook. It is widely used in sunscreen lotion, cream, honey, emulsion, oil and other sunscreen cosmetics as an anti ultraviolet finishing agent. It has good anti-aging and softening effect on cotton fabrics and polyester fibers. It is mainly used as sunscreen in water-soluble cosmetics, UV absorbers in other water-soluble inks and coatings, etc. it is mainly used as sunscreen in water-soluble cosmetics, UV absorbers in other water-soluble inks and coatings, etc.
350 kg water was added to the reactor and 150 kg NaOH was added under stirring. After dissolving, cool down to 10 ℃, add 110kg resorcinol, stir to dissolve. Then 126kg of dimethyl sulfate was added slowly and reacted for 2h at 26-30 ℃. Add water to dilute, separate the oil layer, and wash the oil layer to neutral. Remove the low Buddha point, distill and collect the fraction of 215-220 ℃, i.e. m-phenyldimethyl ether. In the synthesis of 2-hydroxy-4-methoxybenzophenone, 300kg chlorobenzene was firstly added into the condensation reactor, and then the catalyst AlCl3 350 kg and m-phenylene ether 120 kg were added into the reactor under agitation. Heat to about 80 ℃, slowly add 320kg benzoyl chloride. After refluxing for 4-6h, cooling, hydrolysis, steaming out solvent, cooling, crystallization and drying, 2-hydroxy-4-methoxybenzophenone was obtained. In the synthesis of 2-hydroxy-4-methoxy-5-sulfonyldiphenylacetone, 93% sulfuric acid is firstly added into the sulfonation reactor, and then 2-hydroxy-4-methoxydiphenylketone is slowly added under agitation. After reaction at 110 ℃ for 4-6h, the product is cooled, crystallized, dried and recrystallized.